Coulometric Titrator by Karl Fischer's Method PE-9210 is designed for fast and accurate determination of moisture content in a wide range of products and materials in the liquid phase by coulometric titration. The titrator can be used in analytical and chemical technology laboratories, in control and supervision bodies. The device is most convenient for determining moisture in crude oil, heavy petroleum products, diesel fuel, transformer oil, etc. It can be used in laboratory and industrial conditions.
Features:
- The device is listed in the State Register of
Measuring Instruments of the Russian Federation under the number 55135-13;
- The non-diaphragm titration cell is very easy to
operate when cleaned and filled with electrolyte, and its operation requires
only one reagent (anolyte). Ideal for determining a wide range of water
concentrations in samples (from 1000 ppm to 5%)
- The metal case, painted with chemically resistant
paint, reliably protects the device from external influences
- Adaptive titration algorithm guarantees high
accuracy when titrating samples with low moisture content
- The Windows Embedded Compact 7 operating system
installed on the device allows you to save data in the usual Word and Excel
formats;
- Graphical representation of the titration process;
- Built-in methodology for getting started quickly;
- The titration is started by pressing one button;
- Creation and storage of user's techniques in memory
(up to 100 techniques);
- Storing measurement results in memory (up to 1000
series);
- Accounting for the reagent resource;
- RS-232/485 port for connecting scales and
controlling external devices;
- 2 USB B ports for connection to a computer, laser
printer, peripheral input devices (keyboard, mouse);
- The ability to use a USB flash drive (USB flash
drive) to transfer and store data;
- Prompt, high-quality and inexpensive service support
for our users;
Supported standards (GOST, ASTM):
1) ISO 12937:2000 "Petroleum products. Determination
of the water content. Karl Fischer coulometric titration method"
2) GOST R 54284-2010 "Crude oils. Determination
of water by coulometric titration according to Karl Fischer"
3) ASTM D 4928-00 (2010) "Standard Method for the
Determination of Water in Oil by Coulometric Titration according to Karl
Fischer"
4) GOST R 54281-2010 "Petroleum products,
lubricating oils and additives. Method for determining water by coulometric
titration according to Karl Fischer"
5) GOST R IEC 60814 "Determination of moisture in
liquid and solid dielectrics by coulometric titration using an automatic Karl
Fischer titrator"
6) GOST R 56340-2015 "Organic liquids.
Determination of water by coulometric titration according to Karl Fischer"
7) GOST 24614-81 "Liquids and gases that do not
interact with the Fischer reagent. Coulometric method for determining
water"
8) GOST EN 13466-1-2013 "Fertilizers.
Determination of water content (Karl Fischer methods)"
9) GOST 14870-77 "Chemical products. Methods for
determining water"
10) ASTM D
1533-00 «Standard Test Method for Water in Insulating Liquids by Coulometric
Karl Fischer Titration»
11) ASTM E
1064-05 «Standard Test Method for Water in Organic Liquids by Coulometric Karl
Fischer Titration
Technical
specifications:
- The volume of the titration cell is 280 ml;
- Iodine generation in the cell - current pulses of
fixed duration with an amplitude up to 2000 mA;
- Indication of the end point of titration -
alternating current polarization potential;
- Determination of the end point of titration - by
relative drift, by absolute drift or by time;
- The measurement range of the mass of water in the
analyzed sample is from 0.01 to 200 mg;
- The limit of permissible relative error is ± 3.0%;
- The limit of the permissible relative COE of the
random component of the error is 1.5%;
- Sensitivity - 0.1 micrograms of H2O;
- Indication - drift, potential, titration time,
mixing speed;
- Calculations:
a) Automatic calculation of moisture content in ppm,
%, mg, mcg;
b) Automatic drift compensation;
c) Taking into account the result of titration of the
blank sample;
d) Statistical processing of the results of a series
of measurements;
- Agitator - 100-1000 rpm, speed stabilization, step
adjustment;
- Power supply:
Voltage: 198-242 Volts, 50 Hz;
Power
consumption: no more than 170 watts;
- Overall dimensions:
height - no more than 200 mm;
length - no
more than 350 mm;
width - no more
than 275 mm;
- The weight of the titrator is not more than 6.5 kg;
- Service life - 10 years;
- The average operating time is 10,000 hours.
Transport dimensions:
1 box, 350x300x500, weight 8 kg
Basic equipment:
- Fischer titrator – 1 pc.;
- Titrator cell with generator and indicator
electrodes – 1 pc.;
- Molecular sieves – 100 g.;
- Desiccant tube – 1 pc.;
- Anchor for built–in magnetic stirrer - 1 pc.;
- Connecting cables – 1 set;
- Power cable (with grounding) – 1 pc.;
- Needles (for syringe G21) 80 mm – 3 pcs.;
- Sealing lubricant - 10 g;
- Septa – 50 pcs.;
- Operating manual with verification procedure
- Certificate of verification.